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Those familiar with previous editions of Addison
Ault's book will be pleased to see that the sixth edition is still
an excellent text for the introductory organic chemistry
laboratory. There are two main additions to this edition: a
section on waste disposal with subsequent disposal instructions
at the end of each experiment and some new experiments,
most notably several reactions of vanillin.
The section on waste disposal is brief but to the
point. some students may want to know more about what
happens to waste after it leaves their laboratory; perhaps this kind
of information could be added to a future edition. Ault
divides waste into categories that correspond to particular
waste containers: sink, solid waste, nonhalogenated liquid
organic waste, halogenated liquid organic waste, nonhalogenated
solid organic waste, halogenated solid organic waste, and
solid inorganic waste. At the end of each experiment these
categories are listed with the specific materials from the
experiment. The instructions are detailed, but are general enough
to accommodate specific procedures at individual
institutions. This information is a wonderful addition and should
help instructors who have heard one too any times, "What do
I do with this?"
Ault's book is full of experiments that use
"interesting" compounds, compounds with which students are likely
to be familiar. Therefore, the series of vanillin
experiments fits in nicely. The reactions include acetylation,
nitration, bromination, reduction to the alcohol, conversion to
the oxime and semicarbazide, and an aldol condensation.
Also new to this edition are isolation of ibuprofen and
acetylsalicyclic acid from tablets, and trimyristin from nutmeg.
Those who may be new to Ault's text will find a
well-written laboratory manual that clearly reflects the author's
years of experience. It is thorough, describing all the common
lab techniques in Part 1 and giving concise, well-written
directions for experiments in Part 2. The experiments provide
an excellent representation of all the important reactions in a
typical course. In fact, for most types of reactions there are
several experiments from which to choose. Most experiments
are written at the few- to several-gram scale, so that waste is
minimized, but the esthetics of organic chemistry is
maintained. Although microscale techniques are discussed, no
experiments are written specifically for them (except for one exercise).
The book is full of marvelous line drawings for
setups and the layout is such that wide margins are available
for student notes. The author uses these margins to
highlight important points and as a place to point out potential
mistakes, no doubt ones that he has witnessed many
times throughout the years. At the end of nearly every section
there are questions, problems, and/or exercises.
Ault's book is an excellent text. In fact, I look
forward to modifying some of the experiments and using them
with my baby daughter when she is a bit older.
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